CFD Simulation of Capillary Condensation during Freeze Drying of Porous Material

2011 ◽  
Vol 34 (7) ◽  
pp. 1136-1142 ◽  
Author(s):  
M. Hassan Ghajar ◽  
S. H. Hashemabadi
Keyword(s):  
Porous Material ◽  
Freeze Drying ◽  
Cfd Simulation ◽  
Capillary Condensation

scholarly journals Reconstruction of 3D Porous Geometry for Coupled FEM-CFD Simulation

2022 ◽  
Author(s):  
Herman Szűcs
Keyword(s):  
Porous Material ◽  
Numerical Simulations ◽  
Cfd Simulation ◽  
Geometric Model ◽  
Input Parameter ◽  
Complex Process ◽  
Material Sample ◽  
Interaction Simulation ◽  
3D Geometric Model ◽  
Science Material

Porous materials can be found in numerous areas of life (e. g., applied science, material science), however, the simulation of the fluid flow and transport phenomena through porous media is a significant challenge nowadays. Numerical simulations can help to analyze and understand physical processes and different phenomena in the porous structure, as well as to determine certain parameters that are difficult or impossible to measure directly or can only be determined by expensive and time-consuming experiments. The basic condition for the numerical simulations is the 3D geometric model of the porous material sample, which is the input parameter of the simulation. For this reason, geometry reconstruction is highly critical for pore-scale analysis. This paper introduces a complex process for the preparation of the microstructure's geometry in connection with a coupled FEM-CFD two-way fluid-structure interaction simulation. Micro-CT has been successfully applied to reconstruct both the fluid and solid phases of the used porous material.

scholarly journals Structure design and performance analysis of aerostatic thrust bearing with compound restrictors

2022 ◽  
Vol 355 ◽  
pp. 03070
Author(s):  
Yuntang Li ◽  
Yueliang Ye ◽  
Ruirui Li ◽  
Pengfeng Wang ◽  
Fangfang Zhang
Keyword(s):  
Porous Material ◽  
Thrust Bearing ◽  
Cfd Simulation ◽  
Fluid Dynamic ◽  
Structure Design ◽  
Orifice Diameter ◽  
Load Carrying ◽  
Flow Field Characteristics ◽  
Static Performance ◽  
And Performance

Aerostatic thrust bearing compensated by multi-orifices and porous material restrictor simultaneously is proposed to improve the static performance of the bearing. Load Carrying Capacity (LCC), stiffness and the flow field characteristics of the bearing are obtained by Computational Fluid Dynamic (CFD) simulation. The influences of supply pressure, orifice number, orifice diameter, orifice distribution, porous material thickness and permeability coefficient on the bearing performance are analysed. It is indicated that LCC and stiffness of the bearing with compound restrictors are much higher than those of the bearing with porous material restrictor or multi-orifice restrictor if gas film thickness is in rational range. The bearing with compound restrictors has better stability than that of the bearing with multi-orifice restrictor. Moreover, the optimum bearing parameters with compound restrictors are given to improving the performance of aerostatic thrust bearing.

The Structure Design and Fabrication of Drug Releasing Porous Material

2014 ◽  
Vol 887-888 ◽  
pp. 524-528
Author(s):  
Liu Lan Lin ◽  
Yu Jie Lu
Keyword(s):  
Porous Material ◽  
Freeze Drying ◽  
Freezing Temperature ◽  
Solid Content ◽  
Structure Design ◽  
Test Results ◽  
Freeze Dried ◽  
Mean Size ◽  
The Mean ◽  
Bone Repairing

A kind of drug releasing 3D porous material was designed and fabricated, which could used for bone repairing. The β-tricalcium phosphate (β-TCP) material were fabricated through the rapid prototyping (RP) combining with the freeze-drying, where the scaffold-mould was fabricated by RP. The material was fabricated with ball-milled slurry which solid content was 40%, the pre-freezing temperature was-10°C, and then the material was freeze-dried under vacuum environment at-30°C without sintering. The test results showed that the material had good structure pores with the mean size of 150μm through controlling the pre-freezing temperature, and the compressive strength of the samples was 0.216Mpa.

Hysteresis in a Capillary Condensation System

1994 ◽  
Vol 366 ◽  
Author(s):  
M. P. Lilly ◽  
R. B. Hallock
Keyword(s):  
Experimental Data ◽  
Porous Material ◽  
Capillary Condensation ◽  
Hysteretic Behavior ◽  
Preisach Model

ABSTRACTWe report measurements of the hysteretic capillary condensation of liquid 4He into the porous material Nuclepore. Results are presented for global and hysteretic behavior for 300 Å diameter pores. These observations deviate from the predictions of the Preisach model of independent hysteresis domains. By modifying the Preisach model so as to restrict the ability of some of the pores to drain normally we are able to model many features of the experimental data.

Ca-Histochemistry in slime mold plasmodia

1978 ◽  
Vol 36 (2) ◽  
pp. 130-131
Author(s):  
Ulrich Dierkes
Keyword(s):  
Physarum Polycephalum ◽  
Carbon Coating ◽  
Freeze Drying ◽  
Freeze Fracture ◽  
Freeze Substitution ◽  
Uranyl Acetate ◽  
Slime Mold ◽  
Staining Procedure ◽  
Protoplasmic Streaming ◽  
Intracellular Ca

Calcium is supposed to play an important role in the control of protoplasmic streaming in slime mold plasmodia. The motive force for protoplasmic streaming is generated by the interaction of actin and myosin. This contraction is supposed to be controlled by intracellular Ca-fluxes similar to the triggering system in skeleton muscle. The histochemical localisation of calcium however is problematic because of the possible diffusion artifacts especially in aquous media.To evaluate this problem calcium localisation was studied in small pieces of shock frozen (liquid propane at -189°C) plasmodial strands of Physarum polycephalum, which were further processed with 3 different methods: 1) freeze substitution in ethanol at -75°C, staining in 100% ethanol with 1% uranyl acetate, and embedding in styrene-methacrylate. For comparison the staining procedure was omitted in some preparations. 2)Freeze drying at about -95°C, followed by immersion with 100% ethanol containing 1% uranyl acetate, and embedding. 3) Freeze fracture, carbon coating and SEM investigation at temperatures below -100° C.

The Critical Point Drying Method Applied to Scanning Electron Microscopy of L-929 Cells

1970 ◽  
Vol 28 ◽  
pp. 278-279
Author(s):  
Charles TurnbiLL ◽  
Delbert E. Philpott
Keyword(s):  
Electron Microscopy ◽  
Carbon Dioxide ◽  
Surface Tension ◽  
Critical Point ◽  
Freeze Drying ◽  
Attractive Alternative ◽  
Crystal Formation ◽  
Critical Point Drying ◽  
Time Required ◽  
Scanning Electron

The advent of the scanning electron microscope (SCEM) has renewed interest in preparing specimens by avoiding the forces of surface tension. The present method of freeze drying by Boyde and Barger (1969) and Small and Marszalek (1969) does prevent surface tension but ice crystal formation and time required for pumping out the specimen to dryness has discouraged us. We believe an attractive alternative to freeze drying is the critical point method originated by Anderson (1951; for electron microscopy. He avoided surface tension effects during drying by first exchanging the specimen water with alcohol, amy L acetate and then with carbon dioxide. He then selected a specific temperature (36.5°C) and pressure (72 Atm.) at which carbon dioxide would pass from the liquid to the gaseous phase without the effect of surface tension This combination of temperature and, pressure is known as the "critical point" of the Liquid.

Preservation of Plant Cell Surfaces For Scanning Electron Microscopy

1973 ◽  
Vol 31 ◽  
pp. 472-473
Author(s):  
Linda M. Sicko ◽  
Thomas E. Jensen
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Critical Point ◽  
Filter Paper ◽  
Freeze Drying ◽  
Cell Surfaces ◽  
Air Drying ◽  
Popular Method ◽  
Critical Point Drying ◽  
Scanning Electron

The use of critical point drying is rapidly becoming a popular method of preparing biological samples for scanning electron microscopy. The procedure is rapid, and produces consistent results with a variety of samples. The preservation of surface details is much greater than that of air drying, and the procedure is less complicated than that of freeze drying. This paper will present results comparing conventional air-drying of plant specimens to critical point drying, both of fixed and unfixed material. The preservation of delicate structures which are easily damaged in processing and the use of filter paper as a vehicle for drying will be discussed.

Scanning Electron Microscopy-cuticular Lesions on the Roundworm Ascaris Suum

1970 ◽  
Vol 28 ◽  
pp. 114-115
Author(s):  
P. A. Madden ◽  
W. R. Anderson
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Freeze Drying ◽  
Room Temperature ◽  
Secondary Electron ◽  
Distilled Water ◽  
Freeze Dried ◽  
Silver Paint ◽  
To Come ◽  
Scanning Electron

The intestinal roundworm of swine is pinkish in color and about the diameter of a lead pencil. Adult worms, taken from parasitized swine, frequently were observed with macroscopic lesions on their cuticule. Those possessing such lesions were rinsed in distilled water, and cylindrical segments of the affected areas were removed. Some of the segments were fixed in buffered formalin before freeze-drying; others were freeze-dried immediately. Initially, specimens were quenched in liquid freon followed by immersion in liquid nitrogen. They were then placed in ampuoles in a freezer at −45C and sublimated by vacuum until dry. After the specimens appeared dry, the freezer was allowed to come to room temperature slowly while the vacuum was maintained. The dried specimens were attached to metal pegs with conductive silver paint and placed in a vacuum evaporator on a rotating tilting stage. They were then coated by evaporating an alloy of 20% palladium and 80% gold to a thickness of approximately 300 A°. The specimens were examined by secondary electron emmission in a scanning electron microscope.

Video real-time imaging of artificial membranes during freeze-drying by cryo-electron microscopy

1988 ◽  
Vol 46 ◽  
pp. 16-17
Author(s):  
Alan S. Rudolph ◽  
Ronald R. Price
Keyword(s):  
Real Time ◽  
Self Assembly ◽  
Freeze Drying ◽  
Video Capture ◽  
Drying Process ◽  
Artificial Membranes ◽  
The Past ◽  
Cryo Electron Microscopy ◽  
Spherical Structures ◽  
Capture Techniques

We have employed cryoelectron microscopy to visualize events that occur during the freeze-drying of artificial membranes by employing real time video capture techniques. Artificial membranes or liposomes which are spherical structures within internal aqueous space are stabilized by water which provides the driving force for spontaneous self-assembly of these structures. Previous assays of damage to these structures which are induced by freeze drying reveal that the two principal deleterious events that occur are 1) fusion of liposomes and 2) leakage of contents trapped within the liposome [1]. In the past the only way to access these events was to examine the liposomes following the dehydration event. This technique allows the event to be monitored in real time as the liposomes destabilize and as water is sublimed at cryo temperatures in the vacuum of the microscope. The method by which liposomes are compromised by freeze-drying are largely unknown. This technique has shown that cryo-protectants such as glycerol and carbohydrates are able to maintain liposomal structure throughout the drying process.

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