Synthesis and Characterization of a Novel Low-Viscosity Unsaturated Hyperbranched Polyester Resin

2010 ◽  
Vol 34 (1) ◽  
pp. 119-126 ◽  
Author(s):  
D. Zhang ◽  
J. Wang ◽  
T. Li ◽  
A. Zhang ◽  
D. Jia
Keyword(s):  
Polyester Resin ◽  
Synthesis And Characterization ◽  
Hyperbranched Polyester ◽  
Low Viscosity

Synthesis and characterization of hyperbranched poly (sulfone-amine) modified β-cyclodextrin

e-Polymers ◽  
2006 ◽  
Vol 6 (1) ◽  
Author(s):  
Liang Chen ◽  
Peng He ◽  
Zhifeng Jia ◽  
Xinyuan Zhu ◽  
Deyue Yan
Keyword(s):  
Drug Delivery ◽  
Low Cost ◽  
Food Additives ◽  
Synthesis And Characterization ◽  
Good Solubility ◽  
Low Viscosity ◽  
Hyperbranched Poly ◽  
Potential Applications ◽  
Inclusion Ability

AbstractAn economical strategy to prepare hyperbranched poly(sulfone-amine) modified β-cyclodextrins (HPSA-m-CDs) from natural β-cyclodextrin (β-CD) and other commercially available materials has been reported. The final product has many good properties of hyperbranched poly(sulfone-amine)s (good solubility, low viscosity etc.), while its inclusion ability can also be well kept. It is a feasible approach to prepare functionalized modified cyclodextrin at very low cost, and may have potential applications in the fields of catalysis, drug delivery, food additives, etc.

Synthesis and Characterization of Polydimethylsiloxane (PDMS) with Medium Viscosity via Ring-Opening Polymerization

2021 ◽  
Vol 1028 ◽  
pp. 346-351
Author(s):  
Soni Setiadji ◽  
Zulfi Mofa Agasa ◽  
Diba G Auliya ◽  
Fitrilawati ◽  
Norman Syakir ◽  
...  
Keyword(s):  
Ring Opening ◽  
Vitreoretinal Surgery ◽  
High Viscosity ◽  
Ring Opening Polymerization ◽  
Vitreous Humour ◽  
Synthesis And Characterization ◽  
Low Viscosity ◽  
A Value ◽  
Medium Viscosity

Duration of use and injectability are external factors for Polydimethylsiloxane (PDMS) that needs to be considered when PDMS utilized as a vitreous substituted liquid in vitreoretinal surgery. In general, PDMS which has been used as a substitute for vitreous humour is PDMS with a low viscosity in the value about 1000 cSt and a high viscosity at a value of about 5000 cSt. Various deficiencies have been encountered from low and high viscosity of PDMS, causing research to be continued to obtain PDMS which has suitable properties as a substitute for vitreous humour. One of them is research to obtain medium viscosity of PDMS with a viscosity value of about 2000 cSt. Here, we reported synthesis and characterization of PDMS with medium viscosity in ranges from 1800 to 2600 mPas. PDMS was synthesized through Ring-Opening Polymerization (ROP) pathway using the monomer of Octamethylcyclotetrasiloxane (D4) and the chain terminator of Hexamethyldisiloxane (MM). Various concentrations of potassium hydroxide (KOH) of 3, 4, 6 and 8 %(w/v) were applied as initiator to form gel of PDMS. All synthesized PDMS samples were identified to have viscosity values of 1800-2600 mPas, refractive index values of 1.4042-1.4044 and surface tension values of 22-23 mN/m. Meanwhile, the results of Fourier-Transform Infrared (FTIR) measurement showed that the absorption peaks were similar to that of our previous report.

Synthesis and characterization of hybrid films from hyperbranched polyester using a sol-gel process

2013 ◽  
Vol 131 (3) ◽  
pp. n/a-n/a ◽  
Author(s):  
Amélie Houel ◽  
Jocelyne Galy ◽  
Aurélia Charlot ◽  
Jean-François Gérard
Keyword(s):  
Sol Gel ◽  
Synthesis And Characterization ◽  
Hyperbranched Polyester ◽  
Hybrid Films ◽  
Sol Gel Process

Synthesis and Characterization of Carboxyl-Terminated Hyperbranched Polyester

2014 ◽  
Vol 665 ◽  
pp. 327-330
Author(s):  
Shi Jie Niu ◽  
Jian Wang ◽  
Yu Qing Bai ◽  
Ming Tao Run
Keyword(s):  
Glass Transition ◽  
Sodium Acetate ◽  
Succinic Anhydride ◽  
Molar Ratio ◽  
Synthesis And Characterization ◽  
Hydroxyl Groups ◽  
Hyperbranched Polyester ◽  
End Groups ◽  
Lower Glass Transition Temperature

In order to prepare carboxyl-terminated hyperbranched polyester (HBP-COOH), succinic anhydride was used to modify hydroxyl-terminated hyperbranched polyester (HBP-OH), and the influences of the solvents, catalysts and time on the product’s structure were investigated. When THF is used as the solvent, sodium acetate as the catalyst, the molar ratio of succinic anhydride and hydroxyl groups is 3:1, and the reaction time is 6 h at 65°C, the modification extent of the hydroxyl groups is about 99% with about 95% yield. HBP-COOH has much lower glass transition temperature than that of HBP-OH due to its long and flexible end-groups.

Synthesis and characterization of APTMS/melamine cured hyperbranched polyester-epoxy hybrid coatings

2013 ◽  
Vol 76 (10) ◽  
pp. 1402-1412 ◽  
Author(s):  
Shaik Allauddin ◽  
M.K. Akhil Chandran ◽  
Kishore Kumar Jena ◽  
Ramanuj Narayan ◽  
K.V.S.N. Raju
Keyword(s):  
Hybrid Coatings ◽  
Synthesis And Characterization ◽  
Hyperbranched Polyester

Synthesis and Characterization of Low-Viscosity Bio-Based Styrene Alternatives for Bisphenol A Vinyl Ester Thermosetting Resins

2020 ◽  
Vol 8 (46) ◽  
pp. 17234-17244
Author(s):  
John H. Vergara ◽  
Santosh K. Yadav ◽  
Oluwadamilola Bolarin ◽  
John J. La Scala ◽  
Giuseppe R. Palmese
Keyword(s):  
Bisphenol A ◽  
Vinyl Ester ◽  
Synthesis And Characterization ◽  
Thermosetting Resins ◽  
Low Viscosity
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