Insight into Copper-Based Catalysts: Microwave-Assisted Morphosynthesis, In Situ Reduction Studies, and Dehydrogenation of Ethanol

ChemCatChem ◽  
2011 ◽  
Vol 3 (5) ◽  
pp. 839-843 ◽  
Author(s):  
Diogo P. Volanti ◽  
André G. Sato ◽  
Marcelo O. Orlandi ◽  
José M. C. Bueno ◽  
Elson Longo ◽  
...  
POSITRON ◽  
2020 ◽  
Vol 10 (1) ◽  
pp. 34
Author(s):  
Lia Destiarti ◽  
Oktaviardi Bityasmawan Abdillah ◽  
Retno Maharsi ◽  
Octia Floweri ◽  
Ferry Iskandar

In this work, the photocatalytic performance of electrochemically exfoliated graphite (EG) with low copper addition (≤ 5 wt.%) was studied. Composites of EG/Cu/Cu2O were successfully prepared by microwave-assisted in situ reduction method. FTIR spectra of the samples showed that the main functional groups of graphite were detected in the samples. XRD characterization further proved the presence of EG, Cu, and Cu2O in the samples. The higher proportion of Cu2O presented in the samples prepared with a higher amount of Cu2+. SEM analysis showed that Cu2O/Cu particles were homogeneously deposited on the surface of EG. The composites of EG, Cu, and Cu2O with a varied amount of Cu (1 and 5 wt. %) in EG / Cu2+ mixture were examined as photocatalyst in the degradation process of Rhodamine B (RhB). The photocatalytic degradation of RhB was analysed by observing its decolorization within a set time of irradiation. UV-Vis analysis revealed that the degradation of RhB in EG/Cu/Cu2O A and B for 105 minutes was 26 and 35 %, respectively. The result demonstrates that the sample with a larger amount of Cu2O (sample B, Cu 5 wt.%) shows higher photocatalytic activity in the degradation of RhB.


RSC Advances ◽  
2015 ◽  
Vol 5 (67) ◽  
pp. 54460-54470 ◽  
Author(s):  
Salah A. Hassan ◽  
Heba M. Gobara ◽  
Mohamed M. Gomaa ◽  
Rasha S. Mohamed ◽  
Fikry H. Khalil

In this comparative study of dispersion profile-catalytic performance relationships, Pt (of 0.3, 0.6 and 0.9 wt%) was supported on mesoporous silica surface via microwave assisted solution method or rotary chemical evaporation method in the in situ reduction step.


RSC Advances ◽  
2016 ◽  
Vol 6 (105) ◽  
pp. 103482-103490 ◽  
Author(s):  
P. A. Sajid ◽  
S. Shashank Chetty ◽  
S. Praneetha ◽  
A. Vadivel Murugan ◽  
Yogesh Kumar ◽  
...  

In situreduction and microwave-assisted synthesis of Ag/C-dot and Au/C-dot nanohybrids using natural lemon extract for cancer cellular imaging applications.


Water ◽  
2021 ◽  
Vol 13 (5) ◽  
pp. 738
Author(s):  
Nicola Rossi ◽  
Mario Bačić ◽  
Meho Saša Kovačević ◽  
Lovorka Librić

The design code Eurocode 7 relies on semi-probabilistic calculation procedures, through utilization of the soil parameters obtained by in situ and laboratory tests, or by the means of transformation models. To reach a prescribed safety margin, the inherent soil parameter variability is accounted for through the application of partial factors to either soil parameters directly or to the resistance. However, considering several sources of geotechnical uncertainty, including the inherent soil variability, measurement error and transformation uncertainty, full probabilistic analyses should be implemented to directly consider the site-specific variability. This paper presents the procedure of developing fragility curves for levee slope stability and piping as failure mechanisms that lead to larger breaches, where a direct influence of the flood event intensity on the probability of failure is calculated. A range of fragility curve sets is presented, considering the variability of levee material properties and varying durations of the flood event, thus providing crucial insight into the vulnerability of the levee exposed to rising water levels. The procedure is applied to the River Drava levee, a site which has shown a continuous trend of increased water levels in recent years.


2021 ◽  
Vol 9 (1) ◽  
pp. 104889
Author(s):  
Wyllamanney da S. Pereira ◽  
Fabrício B. Destro ◽  
Cipriano B. Gozzo ◽  
Edson R. Leite ◽  
Júlio C. Sczancoski

2021 ◽  
Vol 5 (7) ◽  
pp. 2055-2064
Author(s):  
Saheli Biswas ◽  
Aniruddha P. Kulkarni ◽  
Daniel Fini ◽  
Sarbjit Giddey ◽  
Sankar Bhattacharya

In situ synthesis of methane in a single-temperature zone SOEC in the absence of any methanation catalyst is a completely electrochemical phenomenon governed by the thermodynamic equilibrium of various reactions.


Author(s):  
Xixi Liu ◽  
Yanxin Wang ◽  
Bo Li ◽  
Bing Liu ◽  
Wei Wang ◽  
...  

Author(s):  
Amun Amri ◽  
Ahmad Ainun Najib ◽  
Monita Olivia ◽  
Mohammednoor Altarawneh ◽  
Aman Syam ◽  
...  

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