Liquid chromatography–mass spectrometry applications for quantification of endogenous sex hormones

2020 ◽  
Vol 35 (1) ◽  
Author(s):  
Amy Gravitte ◽  
Timothy Archibald ◽  
Allison Cobble ◽  
Benjamin Kennard ◽  
Stacy Brown
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Sex Hormones ◽  
Liquid Chromatography Mass Spectrometry ◽  
Chromatography Mass Spectrometry ◽  
Endogenous Sex Hormones

scholarly journals Sample Preparation and Liquid Chromatography Mass Spectrometry Analysis of Alkylphenolic Compounds and Steroid Sex Hormones in Sediments

2002 ◽  
Vol 2 ◽  
pp. 1610-1616 ◽  
Author(s):  
Mira Petrovia ◽  
Damia Barcela
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Sex Hormones ◽  
Degradation Products ◽  
Mass Spectrometry Analysis ◽  
Liquid Chromatography Mass Spectrometry ◽  
Spectrometry Analysis ◽  
Chromatography Mass Spectrometry ◽  
Steroid Sex Hormones

A new methodology, based on the use of accelerated solvent extraction (ASE) and highly selective cleanup using restricted access material (RAM) on-line coupled with liquid chromatography–mass spectrometry (LC–MS), is presented for the simultaneous and unequivocal determination of alkylphenol ethoxylates (APEOs), their degradation products and halogenated derivatives, and steroid sex hormones in sediment samples. Using the integrated RAM–LC–MS system, the simultaneous determination of alkylphenolic compounds and sex hormones was achieved, yielding recoveries higher than 60% and producing low MS background noise.

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