One-Pot Synthesis of β-Keto Sulfones by the Condensative Decarboxylation of Sulfonylacetic Acids with Acid Chlorides under Mild Conditions

2015 ◽  
Vol 36 (12) ◽  
pp. 2956-2958 ◽  
Author(s):  
Kieseung Lee
Keyword(s):  
Acid Chlorides ◽  
One Pot ◽  
Mild Conditions ◽  
One Pot Synthesis

scholarly journals One-pot synthesis of polysubstituted indoles from aliphatic nitro compounds under mild conditions

2007 ◽  
Vol 48 (10) ◽  
pp. 1809-1811 ◽  
Author(s):  
Christopher A. Simoneau ◽  
Alexis M. Strohl ◽  
Bruce Ganem
Keyword(s):  
Nitro Compounds ◽  
One Pot ◽  
Aliphatic Nitro Compounds ◽  
Mild Conditions ◽  
One Pot Synthesis

Palladium-Catalyzed One-Pot Stereospecific Synthesis of 2-Deoxy Aryl C-Glycosides from Glycals and Anilines in the Presence of tert-Butyl Nitrite

Synthesis ◽  
2019 ◽  
Vol 51 (22) ◽  
pp. 4215-4230 ◽  
Author(s):  
Adesh Kumar Singh ◽  
Rapelly Venkatesh ◽  
Jeyakumar Kandasamy
Keyword(s):  
Room Temperature ◽  
Stereospecific Synthesis ◽  
One Pot ◽  
Tert Butyl ◽  
Mild Conditions ◽  
One Pot Synthesis ◽  
Palladium Catalyzed ◽  
Aryl Glycosides

The palladium-catalyzed one-pot synthesis of 2,3-deoxy-3-keto aryl C-glycosides is achieved from glycals and anilines in the presence of tert-butyl nitrite and aqueous HBF4 under mild conditions. This one-pot method stereospecifically provides α- and β-aryl glycosides (≥19:1 by NMR) in good yields at room temperature. The configuration at the C-3 position in the glycal determines the anomeric selectivity (i.e., α or β) of the desired products.

Sequential one-pot synthesis of (1→6) amide-linked oligosaccharide mimetics under mild conditions

2020 ◽  
Vol 39 (5-6) ◽  
pp. 267-287
Author(s):  
Shuang Hao ◽  
Shuai Lin ◽  
Xin Wang ◽  
Ran An ◽  
Mengbi Guo ◽  
...  
Keyword(s):  
One Pot ◽  
Mild Conditions ◽  
One Pot Synthesis

A one-pot synthesis of alkyl acylcarbamodithioates from acid chlorides, thiols, and ammonium thiocyanate

2009 ◽  
Vol 140 (10) ◽  
pp. 1199-1204 ◽  
Author(s):  
Issa Yavari ◽  
Nasir Iravani ◽  
S. Zahra Sayyed-Alangi ◽  
Rahimeh Hajinasiri
Keyword(s):  
Ammonium Thiocyanate ◽  
Acid Chlorides ◽  
One Pot ◽  
One Pot Synthesis

scholarly journals One-Pot Synthesis of α-Substituted Acrylates

SynOpen ◽  
2018 ◽  
Vol 02 (02) ◽  
pp. 0161-0167
Author(s):  
Magdalini Matziari ◽  
Yixin Xie
Keyword(s):  
Amino Acids ◽  
Reaction Times ◽  
Synthetic Method ◽  
One Pot ◽  
Biologically Relevant ◽  
Mild Conditions ◽  
One Pot Synthesis ◽  
Acrylic Esters ◽  
Natural Amino Acids ◽  
Work Up

A simple and efficient synthetic method towards α-substituted acrylic esters has been developed using the Horner–Wadsworth–Emmons (HWE) reaction with HCHO after alkylation of phosphonoacetates in a one-pot reaction. This method allows the smooth introduction of various side-chains, such as natural amino acids and other biologically relevant substituents. The use of mild conditions, inexpensive reagents, short reaction times and simple work-up and purification steps provides an effective and general alternative to cumbersome multistep and low-yielding procedures described to date.

One-pot synthesis of polyoxomolybdate anion intercalated layered double hydroxides and their application in ultra-deep desulfurization of fuels under mild conditions

2018 ◽  
Vol 5 (9) ◽  
pp. 2205-2210 ◽  
Author(s):  
Yu Guo ◽  
Jiawei Fu ◽  
Li Li ◽  
Xiaonan Li ◽  
Haiyu Wang ◽  
...  
Keyword(s):  
Layered Double Hydroxides ◽  
One Pot ◽  
Mild Conditions ◽  
One Pot Synthesis ◽  
Deep Desulfurization ◽  
Double Hydroxides ◽  
Sulfur Containing ◽  
Sulfur Containing Compounds

1 mol sulfur-containing compounds can be directly oxidized by 2 mol oxidants into their corresponding sulfones.

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