Acid-catalyzed Synthesis and Characterization of a Nanocrystalline Cobalt-based Prussian Blue Analogs (Co3[Co(CN)6]2·nH2O) by Single-Source Method under Hydrothermal Conditions and Its Conversion to Co3O4

2015 ◽  
Vol 36 (9) ◽  
pp. 2387-2390 ◽  
Author(s):  
Sumin Kang ◽  
Seungbin Im ◽  
Youngjin Jeon
Keyword(s):  
Prussian Blue ◽  
Synthesis And Characterization ◽  
Single Source ◽  
Hydrothermal Conditions ◽  
Source Method ◽  
Acid Catalyzed ◽  
Prussian Blue Analogs

Synthesis and Characterization of Potential Single-Source Precursors to Group 13−Antimonides

1996 ◽  
Vol 15 (23) ◽  
pp. 5035-5038 ◽  
Author(s):  
Ryan A. Baldwin ◽  
Edward E. Foos ◽  
Richard L. Wells ◽  
Peter S. White ◽  
Arnold L. Rheingold ◽  
...  
Keyword(s):  
Synthesis And Characterization ◽  
Single Source ◽  
Group 13 ◽  
Single Source Precursors

Synthesis and Characterization of Calcium Zeolite-Cowlesite.

2021 ◽  
Vol 23 (05) ◽  
pp. 787-790
Author(s):  
Abhijit M ◽  
◽  
Suresh Kumar. B. V ◽  
Keyword(s):  
Low Temperature ◽  
Elemental Concentration ◽  
Stoichiometric Composition ◽  
Lattice Parameter ◽  
Raw Material ◽  
Synthesis And Characterization ◽  
Aluminum Silicate ◽  
Hydrothermal Conditions ◽  
Orthorhombic System

Cowlesite is a Calcium Aluminum silicate CaAl2Si3O106H2O which formed under the hydrothermal conditions of low temperature (1800C) and pressure (1.013250bar). Cowlesite minerals are known for their peculiar occurrence. Synthesis of Cowlesite mineral was carried by suitable stoichiometric composition. Hydrothermal synthesized Cowlesite mineral was characterized by XRD, SEM, and EDAX. It crystallized in the orthorhombic system and a lattice parameter a=23.22Å, b=30.58Å, c=25.01Å, Volume of Unit cell=17758.79Å3, α=β=γ=900. EDAX results show the elemental concentration of raw material which was used.

scholarly journals Characterization of Prussian Blue Analogs of the Type M3[Fe(CN)5CO]2·xH2O

1982 ◽  
Vol 55 (3) ◽  
pp. 733-737 ◽  
Author(s):  
Hidenari Inoue ◽  
Takashi Kawai ◽  
Masaki Nagao ◽  
Saburo Yanagisawa
Keyword(s):  
Prussian Blue ◽  
Prussian Blue Analogs

Synthesis and characterization of ultrathin metal coordination Prussian blue nanoribbons

2013 ◽  
Vol 42 (15) ◽  
pp. 5242 ◽  
Author(s):  
Suping Bao ◽  
Wangping Qin ◽  
Qihua Wu ◽  
Guodong Liang ◽  
Fangming Zhu ◽  
...  
Keyword(s):  
Prussian Blue ◽  
Metal Coordination ◽  
Synthesis And Characterization

Synthesis and characterization of iron tin oxide thin films from single source bimetallic precursors

Polyhedron ◽  
2014 ◽  
Vol 69 ◽  
pp. 40-47 ◽  
Author(s):  
Nasir Khan ◽  
Amin Badshah ◽  
Bhajan Lal ◽  
Muhammad Azad Malik ◽  
James Raftery ◽  
...  
Keyword(s):  
Thin Films ◽  
Tin Oxide ◽  
Synthesis And Characterization ◽  
Single Source ◽  
Oxide Thin Films

Synthesis and characterization of the lead borate Pb6B12O21(OH)6

2016 ◽  
Vol 71 (8) ◽  
pp. 925-933 ◽  
Author(s):  
Sandra Schönegger ◽  
Teresa S. Ortner ◽  
Klaus Wurst ◽  
Gunter Heymann ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
Hydrothermal Synthesis ◽  
Potassium Nitrate ◽  
Lattice Parameters ◽  
Synthesis And Characterization ◽  
Lead Borate ◽  
Hydrothermal Conditions ◽  
Organic Reagents ◽  
Synthesis Conditions

AbstractA lead borate with the composition Pb6B12O21(OH)6 was synthesized through a hydrothermal synthesis, using lead metaborate in combination with sodium nitrate and potassium nitrate. The compound crystallizes in the trigonal, non-centrosymmetric space group P32 (no. 145) with the lattice parameters a = 1176.0(4), c = 1333.0(4) pm, and V = 0.1596(2) nm3. Interestingly, the data of Pb6B12O21(OH)6 correct the structure of a literature known lead borate with the composition “Pb6B11O18(OH)9”. For the latter compound, nearly identical lattice parameters of a = 1176.91(7) and c = 1333.62(12) pm were reported, possessing a crystal structure, in which the localization and refinement of one boron atom was obviously overlooked. The structure of Pb6B12O21(OH)6 is built up from trigonal planar BO3 and tetrahedral BO4 groups forming complex chains. The Pb2+ cations are located between neighboring polyborate chains. The here reported compound Pb6B12O21(OH)6 and “Pb6B11O18(OH)9” were, however, produced under different synthesis conditions. While “Pb6B11O18(OH)9” was synthesized via a hydrothermal synthesis including ethylenediamine and acetic acid, the here reported lead borate Pb6B12O21(OH)6 could be obtained under moderate hydrothermal conditions (240°C) without the addition of organic reagents.

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