Synthesis and characterization of a novel high luminescent gold-2-mercapto-1-methyl-imidazole complex

Luminescence ◽  
2010 ◽  
Vol 26 (6) ◽  
pp. 506-509 ◽  
Author(s):  
Giorgio Cardone ◽  
Gianfranco Carotenuto ◽  
Pellegrino Conte ◽  
Giuseppe Alonzo
Keyword(s):  
Synthesis And Characterization ◽  
Methyl Imidazole

Synthesis and Characterization of Supported on Silica Based Ionic Liquids

2015 ◽  
Vol 727-728 ◽  
pp. 34-37
Author(s):  
Li Ying Guo ◽  
Jun Shi ◽  
Jun Hai He ◽  
Ji Yue Huang ◽  
Peng Cheng Huang
Keyword(s):  
Crystal Structure ◽  
Ionic Liquid ◽  
Ionic Liquids ◽  
Chemical Structure ◽  
Sol Gel ◽  
Synthesis And Characterization ◽  
Imidazolium Ionic Liquid ◽  
Imidazolium Ionic Liquids ◽  
Methyl Imidazole

Three kinds of functionalized imidazolium ionic liquid, 1-chloride (2-hydroxyethyl) -3-methyl imidazole ionic liquid [HeMIM]Cl, 1-bromide ethylamine-3-methyl imidazolium ionic liquid [AeMIM]Br and chlorinated 1-carboxyethyl-3-methyl imidazolium ionic liquid [CeMIM]Cl, were synthesized firstly. Subsequently, three kinds of supported silicon imidazolium ionic liquids were prepared from above ionic liquids with tetraethoxysilane by sol-gel method. The Chemical structure and crystal structure of the supported on silica based ionic liquids were analyzed by FTIR and XRD.

The Synthesis and Characterization of 1-methyl-3-butyl imidazole Tetrafluoroborate

2013 ◽  
Vol 303-306 ◽  
pp. 2640-2643 ◽  
Author(s):  
Peng Tian ◽  
Jing Zeng ◽  
Zhi Gang Zhao ◽  
Bo Meng ◽  
Tian Ling Qin ◽  
...  
Keyword(s):  
Room Temperature ◽  
Forward Direction ◽  
Structure Characterization ◽  
Synthesis And Characterization ◽  
Room Temperature Ionic Liquids ◽  
Synthesis Reaction ◽  
Continuous Precipitation ◽  
Infrared Spectrometer ◽  
Methyl Imidazole

1-methyl-3-butyl Imidazole chloride is prepared by 1–methyl imidazole and chlorinated n-butane. The synthesis reaction of 1-methyl-3-butyl imidazole tetrafluoroborate is in the acetone. The solubility of NaBF4and BMIC in acetone is not large, but due to the insolubility in acetone of reaction product NaCl and continuous precipitation from the liquid phase in the reaction process, so as to promote the reaction continuously towards forward direction. The colorless transparent and odorless BMIBF4are gotten. We use infrared spectrometer for the structure characterization, it is proved that we have gotten BMI-BF4room temperature ionic liquids. BMIC ionic liquid has better solubility in H2O, ethanol, ethyl acetate, acetone, acetonitrile, and methanol, and is insoluble in the ether and cyclohexane.

Synthesis and Characterization of the Three Dicyclopentapyrenes

1996 ◽  
Vol 61 (10) ◽  
pp. 3572-3572
Author(s):  
Lawrence T. Scott ◽  
Atena Necula
Keyword(s):  
Synthesis And Characterization

Synthesis and characterization of TiN / Ti / AISI 410 coatings

2018 ◽  
Vol 2 (1) ◽  
pp. 7
Author(s):  
S Chirino ◽  
Jaime Diaz ◽  
N Monteblanco ◽  
E Valderrama
Keyword(s):  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Columnar Grains ◽  
Tin Thin Films ◽  
Steel Aisi ◽  
Interacting Surfaces ◽  
Stainless Steel Aisi

The synthesis and characterization of Ti and TiN thin films of different thicknesses was carried out on a martensitic stainless steel AISI 410 substrate used for tool manufacturing. The mechanical parameters between the interacting surfaces such as thickness, adhesion and hardness were measured. By means of the scanning electron microscope (SEM) the superficial morphology of the Ti/TiN interface was observed, finding that the growth was of columnar grains and by means of EDAX the existence of titanium was verified.  Using X-ray diffraction (XRD) it was possible to observe the presence of residual stresses (~ -3.1 GPa) due to the different crystalline phases in the coating. Under X-ray photoemission spectroscopy (XPS) it was possible to observe the molecular chemical composition of the coating surface, being Ti-N, Ti-N-O and Ti-O the predominant ones.

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