Effects of different polymerization protocols on the degree of conversion of two dual-cured core buildup composites polymerized by light-emitting diode and halogen light-curing units

2014 ◽  
Vol 131 (15) ◽  
pp. n/a-n/a
Author(s):  
Duygu Karakis ◽  
Arzu Zeynep Yildirim-Bicer ◽  
Ozlem Erol ◽  
Arife Dogan
2007 ◽  
Vol 18 (1) ◽  
pp. 54-59 ◽  
Author(s):  
Cesar Augusto Galvão Arrais ◽  
Fenelon Martinho Pontes ◽  
Luis Presley Serejo dos Santos ◽  
Edson Roberto Leite ◽  
Marcelo Giannini

This study evaluated the effect of blue light emitting diode (LED) and quartz tungsten halogen (QTH) on the degree of conversion (DC) of an etch-and-rinse Single Bond adhesive system (SB) and a mixture composed of primer solution and resin bond from Clearfil SE Bond self-etching adhesive system (CB) using Fourier transform infrared analysis (FTIR). Adhesives were applied to potassium bromide pellet surfaces and FTIR analyses were performed before and after photo-activation for 10 s with either LED (Freelight 1 - 400 mw/cm²) or QTH (XL 3000 - 630 mw/cm²) light-curing units (n=8). Additional FTIR spectra were obtained from photo-activated samples stored in distilled water for 1 week. The DC was calculated by comparing the spectra obtained from adhesive resins before and after photo-activation. The results were analyzed by two-way split-plot ANOVA and Tukey's test (p<0.05). Both adhesive systems exhibited low DC (%) immediately after photo-activation (SB/QTH: 18.7 ± 3.9; SB/LED: 13.5 ± 3.3; CF/QTH: 13.6 ± 1.9; CF/LED: 6.1 ± 1.0). The DC of samples light-cured with LED was lower than DC of those light-cured with QTH, immediately after light curing and after 1 week (SB/QTH: 51.3 ± 6.6; SB/LED: 50.3 ± 4.8; CF/QTH: 56.5 ± 2.9; CF/LED: 49.2 ± 4.9). The LED curing unit used to photo-activate the adhesive resins promoted lower DC than the QTH curing unit both immediately after light curing and 1 week after storage in water.


2009 ◽  
Vol 79 (1) ◽  
pp. 144-149 ◽  
Author(s):  
Mustafa Ulker ◽  
Tancan Uysal ◽  
Sabri Ilhan Ramoglu ◽  
Huseyin Ertas

Abstract Objective: To compare the microleakage of the enamel-adhesive-bracket complex at the occlusal and gingival margins of brackets bonded with high-intensity light curing lights and conventional halogen lights. Materials and Methods: Forty-five freshly extracted human maxillary premolar teeth were randomly separated into three groups of 15 teeth each. Stainless steel brackets were bonded in all groups according to the manufacturer's recommendations. Specimens (15 per group) were cured for 40 seconds with a conventional halogen light, 20 seconds with light-emitting diode (LED), and 6 seconds with plasma arc curing light (PAC). After curing, the specimens were further sealed with nail varnish, stained with 0.5% basic-fuchsine for 24 hours, sectioned and examined under a stereomicroscope, and scored for microleakage for the enamel-adhesive and bracket-adhesive interfaces from both the occlusal and gingival margins. Statistical analyses were performed using Kruskal-Wallis and Mann-Whitney U-tests with a Bonferroni correction. Results: The type of light curing unit did not significantly affect the amount of microleakage at the gingival or occlusal margins of investigated interfaces (P &gt;.05). The gingival sides in the LED and PAC groups exhibited higher microleakage scores compared with those observed on occlusal sides for the enamel-adhesive and adhesive-bracket interfaces. The halogen light source showed similar microleakage at the gingival and occlusal sides between both adhesive interfaces. Conclusions: High-intensity curing units did not cause more microleakage than conventional halogen lights. This supports the use of all these curing units in routine orthodontic practice.


Author(s):  
Anuradha Vitthal Wankhade ◽  
Sharad Basavraj Kamat ◽  
Santosh Irappa Hugar ◽  
Girish Shankar Nanjannawar ◽  
Sumit Balasaheb Vhate

Introduction: New generation composite resin materials have revolutionized the art of aesthetic dentistry. The clinical success is dependent on effective polymerisation and surface hardness which in turn are dependent on the performance of Light Curing Units (LCU). This study utilises surface hardness as a measure of degree of polymerisation of composite resins achieved by LCUs. Aim: To evaluate the difference in surface hardness of nanohybrid and microhybrid resin composites cured by light curing systems, Light Emitting Diode (LED) and Quartz Tungsten Halogen (QTH). Materials and Methods: In this invitro experimental study, two types of hybrid composites (Nanohybrid and Microhybrid) were tested for surface hardness by using two different light curing systems (LED and QTH). All the Nanohybrid and Microhybrid specimens were cured using LED and QTH LCUs, thus giving four combinations. A total of 60 specimens (6 mm diameter and 2 mm depth) were prepared using Teflon mould with 15 samples for each combination. Surface hardness was measured on upper and lower surface after 24 hours and hardness ratio was calculated. Data was analysed using independent t-test for intergroup comparison. Level of significance was kept at 5%. Results: Surface hardness of resin composites cured by LED LCU was greater than those cured by QTH LCU. Additionally, the hardness value was greater for the upper surface. Nanohybrids showed better surface hardness than Microhybrids for both the LCUs. Conclusion: Nanohybrid composite resins and LED system were found to be more effective in terms of surface hardness as compared to their counterparts.


2019 ◽  
Vol 44 (3) ◽  
pp. E133-E144 ◽  
Author(s):  
AO Al-Zain ◽  
GJ Eckert ◽  
JA Platt

SUMMARY Objectives: To investigate the influence of curing distance on the degree of conversion (DC) of a resin-based composite (RBC) when similar radiant exposure was achieved using six different light-curing units (LCUs) and to explore the correlation among irradiance, radiant exposure, and DC. Methods and Materials: A managing accurate resin curing-resin calibrator system was used to collect irradiance data for both top and bottom specimen surfaces with a curing distance of 2 mm and 8 mm while targeting a consistent top surface radiant exposure. Square nanohybrid-dual-photoinitiator RBC specimens (5 × 5 × 2 mm) were cured at each distance (n=6/LCU/distance). Irradiance and DC (micro-Raman spectroscopy) were determined for the top and bottom surfaces. The effect of distance and LCU on irradiance, radiant exposure, and DC as well as their linear associations were analyzed using analysis of variance and Pearson correlation coefficients, respectively (α=0.05). Results: While maintaining a similar radiant exposure, each LCU exhibited distinctive patterns in decreased irradiance and increased curing time. No significant differences in DC values (63.21%-70.28%) were observed between the 2- and 8-mm distances, except for a multiple-emission peak LCU. Significant differences in DC were detected among the LCUs. As expected, irradiance and radiant exposure were significantly lower on the bottom surfaces. However, a strong correlation between irradiance and radiant exposure did not necessarily result in a strong correlation with DC. Conclusions: The RBC exhibited DC values &gt;63% when the top surface radiant exposure was maintained, although the same values were not reached for all lights. A moderate-strong correlation existed among irradiance, radiant exposure, and DC.


2013 ◽  
Vol 1 (1) ◽  
pp. 91
Author(s):  
Anderson Catelan ◽  
Caetano Tamires ◽  
Boniek Castillo Dutra Borges ◽  
Giulliana Panfiglio Soares ◽  
Bruno de Castro Ferreira Barreto ◽  
...  

Adequate physical properties of the resinous materials are related to clinical longevity of adhesive restorations. The aim of this investigation was to assess the impact of light-curing source and curing time on the degree of conversion (DC) and Knoop hardness number (KHN) of a composite resin. Circular specimens (5 x 2 mm) were carried out (n = 7) of the Filtek Z250 (3M ESPE) composite. The specimens were light-cured by quartz-halogen-tungsten (QTH) XL 3000 (3M ESPE, 450 mW/cm2) or light-emitting diode (LED) Bluephase 16i (Vivadent, 1390 mW/cm2) for 20, 40, or 60 s. After 24 h, absorption spectra of composite were obtained using Spectrum 100 Optica (Perkin Elmer) FT-IR spectrometer in order to calculate the DC and, KHN was performed in the HMV-2T (Shimadzu) microhardness tester under 50-g load for 15 s dwell time. DC and KHN data were subjected to 2-way ANOVA and Tukey’s test at a pre-set alpha of 0.05. The LED showed highest DC and KHN values than QTH (p < 0.05). The increase of curing time improved the DC and KHN, all curing times with statistical difference (p < 0.05). The use of light-curing units with high irradiance and/or the time of cure increased may improve the physical properties of resin-based materials.


2009 ◽  
Vol 32 (1) ◽  
pp. 83-86 ◽  
Author(s):  
G. P. Cerveira ◽  
T. B. Berthold ◽  
A. A. Souto ◽  
A. M. Spohr ◽  
E. M. Marchioro

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