Characterization of the cure of TGDDM/DDS epoxy resins by chemiluminescence I. Spectral and thermal analysis

1987 ◽  
Vol 33 (7) ◽  
pp. 2281-2292 ◽  
Author(s):  
G. A. George ◽  
D. P. Schweinsberg
Keyword(s):  
Thermal Analysis ◽  
Epoxy Resins

Synthesis and characterization of some polyimide-epoxy composites

e-Polymers ◽  
2011 ◽  
Vol 11 (1) ◽  
Author(s):  
Toheed Akhter ◽  
Humaira Masood Siddiqi ◽  
Zareen Akhter ◽  
M. Saeed Butt
Keyword(s):  
Thermal Behavior ◽  
Epoxy Resins ◽  
Analytical Techniques ◽  
Char Yield ◽  
Epoxy Composites ◽  
Hydroxyl Group ◽  
Synthesis And Characterization ◽  
Tetracarboxylic Acid ◽  
Epoxy Amine

AbstractComposites from some novel polyimide and commercial epoxy were prepared aiming to improve the thermal behavior of epoxy resins. Two diamines namely 4-4'-diamino-4''-hydroxytriphenyl methane (DHTM) and 4-4'- diaminotriphenyl methane (DTM) were synthesized by reacting aniline and aldehydes according to a reported method. The synthesized diamines were blended with commercially available epoxy 1, 4-butanedioldiglycidylether (BDDE) to synthesize model epoxy amine networks which were compared with polyimideepoxy composites. The polyimides were synthesized by reaction of these diamines with aromatic anhydride namely 3,3',4,4'-benzophenone tetracarboxylic acid dianhydride (BTDA). These synthesized polyimides were dispersed in epoxy diamine networks to prepare composites. All the monomers and composites were characterized by making use of various analytical techniques including FTIR, NMR, TGA, DSC and XRD. Presence of hydroxyl group in the diamine helped in better dispersion of polyimide leading to high Tg and high char yield at 600 °C.

scholarly journals Synthesis and characterization of PEDMCD as a flame retardant and its application in epoxy resins

RSC Advances ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 2756-2766
Author(s):  
Yi Zhang ◽  
Weiwei Yang
Keyword(s):  
Flame Retardant ◽  
Epoxy Resins ◽  
Synthesis And Characterization ◽  
Direct Polycondensation ◽  
Polycondensation Reaction ◽  
Highly Effective

In this study, a highly effective flame retardant agent, called polybicyclopentaerythritol phosphate-O-4-imino-p-phenylmethane-4-imino-2-chloro-1,3,5-s-triazine (PEDMCD), has been prepared through a direct polycondensation reaction.

Contribution of thermal analysis in the characterization of lime-based mortars with oxblood addition

2019 ◽  
Vol 678 ◽  
pp. 178303 ◽  
Author(s):  
Kun Zhang ◽  
Alberto Grimoldi ◽  
Laura Rampazzi ◽  
Antonio Sansonetti ◽  
Cristina Corti
Keyword(s):  
Thermal Analysis

scholarly journals Synthesis and characterization of the Bi2-xHox/2Zr3x/8O3 compounds

2011 ◽  
Vol 47 (2) ◽  
pp. 105-112 ◽  
Author(s):  
P. Sulcová ◽  
P. Bystrzycki ◽  
L. Válek ◽  
M. Trojan
Keyword(s):  
Thermal Analysis ◽  
Metal Ions ◽  
Powder Diffraction ◽  
Synthesis And Characterization ◽  
Inorganic Pigments

A series of novel environmentally inorganic pigments based on Bi2O3 doped by metal ions such as Zr4+ and Ho3+ have been developed and characterized using of methods of thermal analysis, Xray powder diffraction and CIE L

scholarly journals Characterization of poled and non-poled β-PVDF films using thermal analysis techniques

2004 ◽  
Vol 424 (1-2) ◽  
pp. 201-207 ◽  
Author(s):  
V. Sencadas ◽  
S. Lanceros-Méndez ◽  
J.F. Mano
Keyword(s):  
Thermal Analysis ◽  
Analysis Techniques ◽  
Thermal Analysis Techniques

scholarly journals Stability evaluation of tocopheryl acetate and ascorbyl tetraisopalmitate in isolation and incorporated in cosmetic formulations using thermal analysis

2010 ◽  
Vol 46 (1) ◽  
pp. 129-134 ◽  
Author(s):  
Mariana Mandelli de Almeida ◽  
Cibele Rosana Ribeiro de Castro Lima ◽  
Joyce Santos Quenca-Guillen ◽  
Elder Moscardini Filho ◽  
Lucildes Pita Mercuri ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Raw Materials ◽  
Skin Aging ◽  
Tocopheryl Acetate ◽  
Stability Evaluation ◽  
Scanning Calorimetry ◽  
Cosmetic Formulations ◽  
Cosmetic Formulation ◽  
Excellent Tool

In view of the increase in the number of cosmetic preparations containing antioxidant vitamins, chiefly, due to their action in preventing the process of skin aging, there is a need to develop pre-formulation studies and to validate analytical methods in order to obtain high quality products. Thus, the objective of this research was to evaluate and compare the thermal behavior of tocopheryl acetate and ascorbyl tetraisopalmitate as raw materials, and incorporated into a base cream. Thermogravimetry (TG / DTG) and differential scanning calorimetry (DSC) were used for this purpose. Both vitamins were found to be stable up to 250ºC. The base cream (placebo) and the sample (base cream containing the vitamins) presented different weight loss. Thermal analysis has shown itself to be an excellent tool for the characterization of these vitamins and can be used in routine analysis for quality control of this type of cosmetic formulation.

scholarly journals Characterization of native and oxidized starches of two varieties of Peruvian carrot (Arracacia xanthorrhiza, B.) from two production areas of Paraná state, Brazil

2009 ◽  
Vol 52 (3) ◽  
pp. 701-713 ◽  
Author(s):  
Luciana Shizue Matsuguma ◽  
Luiz Gustavo Lacerda ◽  
Egon Schnitzler ◽  
Marco Aurélio da Silva Carvalho Filho ◽  
Célia Maria Landi Franco ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Reducing Power ◽  
Blue Color ◽  
Carboxyl Content ◽  
Modified Starches ◽  
Physicochemical Methods ◽  
Partial Degradation ◽  
Almost All ◽  
Production Areas

Two commercial varieties of Peruvian carrot ('Amarela de Carandaí' and 'Senador Amaral') were processed into flour, starch and bagasse and chemically evaluated. The starch was extracted, modified with H2O2 and characterized by the physicochemical methods. By using the methylene blue dyeing, the granules of the modified starches showed intense blue color. The carboxyl content, the reducing power and the amount of the water liberated from the pastes after the freeze-thawing were higher for the oxidized starches and their pastes were clearer than those of the native starches of the two varieties from the two production areas. The RVA viscoamylography showed that the modified starches had lower viscosities with differences between the varieties. In the thermal analysis, the temperatures of the pyrolysis were higher for the native (310.37, 299.08, 311.18 ºC) than for the modified starches (294.16, 296.65 e 293.29 ºC) for both the varieties. This difference could be related with the larger surface of the granules due to the partial degradation promoted by the chemical modification. In almost all results, the differences were evident between the varieties but not for the cultivation places.

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