Working Methods Paper: Certification of methylmercury compounds concentration in marine sediment reference material, IAEA-356

1994 ◽  
Vol 8 (6) ◽  
pp. 533-540 ◽  
Author(s):  
M. Horvat ◽  
V. Mandi? ◽  
L. Liang ◽  
N. S. Bloom ◽  
S. Padberg ◽  
...  
Keyword(s):  
Reference Material ◽  
Marine Sediment ◽  
Methylmercury Compounds ◽  
Sediment Reference Material

Preparation and analysis of a marine sediment reference material for the determination of trace organic constituents

1990 ◽  
Vol 338 (4) ◽  
pp. 501-514 ◽  
Author(s):  
Michele M. Schantz ◽  
Bruce A. Benner ◽  
Stephen N. Chesler ◽  
Barbara J. Koster ◽  
Karen E. Hehn ◽  
...  
Keyword(s):  
Reference Material ◽  
Marine Sediment ◽  
Organic Constituents ◽  
Sediment Reference Material ◽  
Trace Organic

Determination of total chromium in Marine Sediment Reference Material BCSS-1

1996 ◽  
Vol 356 (7) ◽  
pp. 416-419
Author(s):  
J. Liu> ◽  
R. E. Sturgeon ◽  
V. J. Boyko ◽  
S. N. Willie
Keyword(s):  
Reference Material ◽  
Marine Sediment ◽  
Total Chromium ◽  
Sediment Reference Material

scholarly journals Validation of Total Mercury in Marine Sediment and Biological Samples, Using Cold Vapour Atomic Absorption Spectrometry

2018 ◽  
Vol 1 (3) ◽  
pp. 31 ◽  
Author(s):  
Ahmed Elezz ◽  
Hassan Mustafa Hassan ◽  
Hamood Abdulla Alsaadi ◽  
Ahmed Easa ◽  
Saeed Al-Meer ◽  
...  
Keyword(s):  
Trace Elements ◽  
Reference Material ◽  
Atomic Absorption Spectrometry ◽  
Atomic Absorption ◽  
Marine Sediment ◽  
Environmental Samples ◽  
Total Mercury ◽  
Absorption Spectrometry ◽  
Freeze Dried ◽  
Cold Vapour

A method for the measurement of total mercury (T-Hg) in environmental samples using cold vapour atomic absorption spectrometry (CV AAS) has been validated yielding a dynamic range (0.04–10.00 μg/kg) and high certified reference material (CRM) recovery (>90%). The validation was carried out according to International Union of Pure and Applied Chemistry (IUPAC) validation and Eurachem Guides. A freeze-dried and homogenised sample was weighed and then digested using Suprapur acids (HNO3, H2SO4, and HF) with potassium dichromate solution in a hot block digestion system. A calibration curve was constructed (R2 > 0.999). Two CRMs (Marine Sediment Reference Material (PACS-3) and Trace Elements in Muscle Tissue (Trace Elements and Methylmercury in Mussel Tissue (NIST2976)) were utilised for quality assurance and control. The limit of quantification (LOQ) calculated as 0.04 µg/kg, and uncertainty (U) calculated as 2%. The obtained results showed the suitability of this method for direct mercury measurement in environmental samples. Additionally, the proficiency of this method was recognised by accreditation under the standard of International Organization for Standardization (ISO/IEC 17025:2017) for competence of testing and calibration laboratories.

New Arctic Marine Sediment Certified Reference Material for Elemental Analysis

2019 ◽  
Vol 52 (3) ◽  
pp. 401-410 ◽  
Author(s):  
Chunxue Xu ◽  
Yaping Wang ◽  
Ziyi An ◽  
Qian Wang ◽  
Dezhong Sun ◽  
...  
Keyword(s):  
Reference Material ◽  
Certified Reference Material ◽  
Elemental Analysis ◽  
Marine Sediment
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