Synthesis of pyrazolopyrimidines in mild conditions by gold nanoparticles supported on magnetic ionic gelation in aqueous solution

2020 ◽  
Vol 34 (7) ◽  
Author(s):  
Lanlan Yu ◽  
Shilong Xing ◽  
Kai Zheng ◽  
Seyed Mohsen Sadeghzadeh
Molecules ◽  
2021 ◽  
Vol 26 (7) ◽  
pp. 1897
Author(s):  
Hideyasu China ◽  
Nami Kageyama ◽  
Hotaka Yatabe ◽  
Naoko Takenaga ◽  
Toshifumi Dohi

We report a convenient and practical method for the preparation of nonexplosive cyclic hypervalent iodine(III) oxidants as efficient organocatalysts and reagents for various reactions using Oxone® in aqueous solution under mild conditions at room temperature. The thus obtained 2-iodosobenzoic acids (IBAs) could be used as precursors of other cyclic organoiodine(III) derivatives by the solvolytic derivatization of the hydroxy group under mild conditions of 80 °C or lower temperature. These sequential procedures are highly reliable to selectively afford cyclic hypervalent iodine compounds in excellent yields without contamination by hazardous pentavalent iodine(III) compound.


2016 ◽  
Vol 27 (2) ◽  
pp. 643-649 ◽  
Author(s):  
Xiao-Yu Wang ◽  
Cheng-Gang Niu ◽  
Li-Juan Guo ◽  
Liu-Yin Hu ◽  
Sheng-Quan Wu ◽  
...  

2018 ◽  
Vol 24 (5) ◽  
pp. 401-414
Author(s):  
Jinsheng Sun ◽  
Guangxin Liu ◽  
Sheng Fu ◽  
Fang Cai ◽  
Hong Yin ◽  
...  

2017 ◽  
Vol 1 (2) ◽  
Author(s):  
Braja Gopal Bag ◽  
Shib Shankar Dash ◽  
Anup Mandal

The antioxidant efficacy of the rhizome extract of Polygonatum cirrhifolium (Mahameda) has been studied against a stable 2, 2-diphenylpicrylhydrazyl (DPPH) radical at room temperature. The chemical constituents present in the rhizome extract have been utilized for the one step synthesis of stable gold nanoparticles at room temperature under very mild conditions.


2012 ◽  
Vol 48 (37) ◽  
pp. 4459 ◽  
Author(s):  
Yuangen Wu ◽  
Shenshan Zhan ◽  
Faze Wang ◽  
Lan He ◽  
Wenting Zhi ◽  
...  

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