Epoxide Speciation and Functional Group Distribution in Graphene Oxide Paper-Like Materials

2012 ◽  
Vol 22 (18) ◽  
pp. 3950-3957 ◽  
Author(s):  
Adrian Hunt ◽  
Dmitriy A. Dikin ◽  
Ernst Z. Kurmaev ◽  
Teak D. Boyko ◽  
Paul Bazylewski ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Functional Group ◽  
Graphene Oxide Paper ◽  
Group Distribution

scholarly journals X-ray Photoelectron Spectroscopy Analysis of Chitosan–Graphene Oxide-Based Composite Thin Films for Potential Optical Sensing Applications

Polymers ◽  
2021 ◽  
Vol 13 (3) ◽  
pp. 478
Author(s):  
Wan Mohd Ebtisyam Mustaqim Mohd Daniyal ◽  
Yap Wing Fen ◽  
Silvan Saleviter ◽  
Narong Chanlek ◽  
Hideki Nakajima ◽  
...  
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Graphene Oxide ◽  
Photoelectron Spectroscopy ◽  
Functional Group ◽  
Optical Sensing ◽  
Composite Thin Films ◽  
Cobalt Ions ◽  
X Ray ◽  
Sensing Applications

In this study, X-ray photoelectron spectroscopy (XPS) was used to study chitosan–graphene oxide (chitosan–GO) incorporated with 4-(2-pyridylazo)resorcinol (PAR) and cadmium sulfide quantum dot (CdS QD) composite thin films for the potential optical sensing of cobalt ions (Co2+). From the XPS results, it was confirmed that carbon, oxygen, and nitrogen elements existed on the PAR–chitosan–GO thin film, while for CdS QD–chitosan–GO, the existence of carbon, oxygen, cadmium, nitrogen, and sulfur were confirmed. Further deconvolution of each element using the Gaussian–Lorentzian curve fitting program revealed the sub-peak component of each element and hence the corresponding functional group was identified. Next, investigation using surface plasmon resonance (SPR) optical sensor proved that both chitosan–GO-based thin films were able to detect Co2+ as low as 0.01 ppm for both composite thin films, while the PAR had the higher binding affinity. The interaction of the Co2+ with the thin films was characterized again using XPS to confirm the functional group involved during the reaction. The XPS results proved that primary amino in the PAR–chitosan–GO thin film contributed more important role for the reaction with Co2+, as in agreement with the SPR results.

Synthesis of Oxygen Functional Group-Controlled Monolayer Graphene Oxide

2021 ◽  
Vol 94 (9) ◽  
pp. 2195-2201
Author(s):  
Tatsuki Tsugawa ◽  
Kazuto Hatakeyama ◽  
Junko Matsuda ◽  
Michio Koinuma ◽  
Shintaro Ida
Keyword(s):  
Graphene Oxide ◽  
Functional Group ◽  
Monolayer Graphene ◽  
Oxygen Functional Group
Sign in / Sign up

Export Citation Format

Share Document